J. Mohrig – Laboratory Techniques in Organic Chemistry (2014)

Автор: J. Mohrig
Название книги: Laboratory Techniques in Organic Chemistry
Формат: PDF
Жанр: Химия
Страницы: 556
Качество: Изначально компьютерное, E-book

Laboratory Techniques in Organic Chemistry is the most comprehensive and detailed presentation of the lab techniques organic chemistry students need to know. Compatible with any organic chemistry lab manual or set of experiments, it combines specific instructions for three different kinds of laboratory glassware: miniscale, standard taper microscale, and Williamson microscale. It is written to provide effective support for guided-inquiry and design-based experiments and projects, as well as for traditional lab experiments.
Contents
Introduction to the Organic Laboratory Essay:—the role of the Laboratory
Safety in the Laboratory
Green Chemistry
Laboratory Notebooks and Prelab Information
Carrying out Chemical Reactions Essay:—Learning to do Organic Chemistry
Laboratory Glassware
Measurements and Transferring Reagents
Heating and Cooling Methods
Setting up Organic Reactions
Computational Chemistry
Basic Methods For Separation, Purification, And Analysis: ESSAY—Intermolecular Forces in Organic Chemistry
Filtration
Extraction
Drying organic Liquids and recovering reaction Products
Boiling Points and Distillation
Refractometry
Melting Points and Melting ranges
Recrystallization
Sublimation
Optical Activity and Enantiomeric Analysis
Chromatography: ESSAY—Modern Chromatographic Separations
Thin-Layer Chromatography
Liquid Chromatography
Gas Chromatography
Spectrometric Methods: ESSAY—the Spectrometric Revolution
Infrared Spectroscopy
Nuclear Magnetic Resonance Spectroscopy
13C and two-Dimensional NMR Spectroscopy
Mass Spectrometry
Ultraviolet and Visible Spectroscopy
Integrated Spectrometry Problems
Designing and Carrying out Organic Experiments: ESSAY—Inquiry-Driven Lab Experiments
Designing Chemical reactions
Using the Literature of Organic Chemistry